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Production of Bauxite Certified Reference Material (BARC-B1201) for Nine Property Values (Al2O3, Fe2O3, SiO2, TiO2, V2O5, MnO, Cr2O3, MgO and LOI) Traceable to SI Units
Geostandards and Geoanalytical Research ( IF 3.8 ) Pub Date : 2023-02-18 , DOI: 10.1111/ggr.12483
Durga Prasad Ankam 1 , Lori Rastogi 1 , V.K. Verma 2 , V. Krishna Kumari 2 , S. Yadlapalli 3 , Kulamani Dash 1, 4
Affiliation  

The National Centre for Compositional Characterisation of Materials (NCCCM) / Bhabha Atomic Research Centre (BARC) and National Aluminium Company Limited (NALCO), India have produced an Indian origin bauxite certified reference material (CRM), referred to as BARC-B1201, certified for major (Al2O3, Fe2O3, SiO2, TiO2, loss on ignition - LOI) and trace contents (V2O5, MnO, Cr2O3, MgO). Characterisation was undertaken by strict adherence to ISO Guides. A method previously developed and validated in our laboratory, using single step bauxite dissolution and subsequent quantitation (of Al2O3, Fe2O3, SiO2, TiO2, V2O5, MnO, Cr2O3 and MgO) by ICP-AES (SSBD ICP-AES) was used for homogeneity studies and an inter-laboratory comparison exercise (ILCE) of the candidate CRM. LOI was determined by thermo-gravimetric analysis. Property values were assigned after an ILCE with participation from seventeen reputed government and private sector laboratories in India. The CRM was certified for nine property values: Al2O3, Fe2O3, SiO2, TiO2, V2O5, MnO, Cr2O3, MgO and LOI, which are traceable to SI units.

中文翻译:

铝土矿标准物质 (BARC-B1201) 的九种特性值(Al2O3、Fe2O3、SiO2、TiO2、V2O5、MnO、Cr2O3、MgO 和 LOI)的生产可追溯至 SI 单位

印度国家材料成分表征中心(NCCCM)/巴巴原子研究中心(BARC)和印度国家铝业有限公司(NALCO)生产了印度原产铝土矿认证参考材料(CRM),简称BARC-B1201,通过认证主要含量(Al 2 O 3、Fe 2 O 3、SiO 2、TiO 2、烧失量 - LOI)和微量含量(V 2 O 5、MnO、Cr 2 O 3,氧化镁)。表征是严格遵守 ISO 指南进行的。我们实验室之前开发和验证的方法,使用一步铝土矿溶解和后续定量(Al 2 O 3、 Fe 2 O 3、 SiO 2、 TiO 2、 V 2 O 5 、 MnO 、 Cr 2 O 3 )ICP-AES (SSBD ICP-AES) 用于候选 CRM 的同质性研究和实验室间比较练习 (ILCE)。LOI 通过热重分析测定。在印度 17 个知名政府和私营部门实验室参与的 ILCE 后,对财产价值进行了分配。CRM 获得了九个属性值的认证:Al 2 O 3、Fe 2 O 3、SiO 2、TiO 2、V 2 O 5 、 MnO、Cr 2 O 3、MgO 和 LOI,这些值可追溯到 SI 单位。
更新日期:2023-02-18
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