Novel nanocomposite MXene/CeCr₂O₄ had been synthesized by means of inexpensive co-precipitation method. This paper reports the smooth nanocomposite of MXene/CeCr₂O₄ by co-precipitation method and the sol–gel route used for spinel cerium chromite (CeCr₂O${}_4)$ nanoparticles in which ethylene glycol chemical is exploited to restrain the accumulation of nanoparticles. The results show the formation of small nanoparticles with an average crystal crystalline size of CeCr₂O₄, MXene, MXene/CeCr₂O₄ nanocomposite is 37.9$$nm, 18.4$$nm, 11.15 nm, respectively. Characterizations, such as the X-ray diffraction (XRD), have demonstrated the amorphous nature of nanocomposite. The structural morphology [scanning electron microscopy (SEM)] shows the formation of nanocomposite with average particle size of$$nm of about 0.59$$nm. Raman spectroscopy shows that chemical bonding, energy dispersive spectroscopy (EDS) and photoluminance spectroscopy were performed and 3.56$$eV is band gap energy calculated from UV spectra. A comprehensive peak was noticed at 1425$$cm${}^{-1}$ because of bending and stretching oscillations of O–H groups and zeta potential value$=-$19.1$$mV. All of these results confirmed the successful formation of nanocomposite of MXene/CeCr₂O₄. The resulting MXene/CeCr₂O₄ nanocomposite structure shows evidence of significant characteristics as compared to single material having much potential for numerous applications such as optical, energy storing and conductive applications.

采用廉价的共沉淀法合成了新型纳米复合材料MXene/CeCr ₂ O _{4 。}本文报道了_通过共沉淀法和用于尖晶石亚铬铁矿（CeCr ₂ O${}_4）$纳米颗粒，其中利用乙二醇化学物质来抑制纳米颗粒的积累。_{结果表明，CeCr 2} O ₄、MXene、MXene/CeCr ₂ O ₄纳米复合材料形成了小纳米粒子，其平均晶粒尺寸为37.9$$纳米，18.4$$分别为11.15 nm、11.15 nm。X 射线衍射 (XRD) 等表征已证明纳米复合材料的无定形性质。结构形态[扫描电子显微镜（SEM）]显示形成了平均粒径为$$纳米约0.59$$纳米。拉曼光谱显示进行了化学键合、能量色散光谱（EDS）和光致发光光谱分析，3.56$$eV 是根据紫外光谱计算的带隙能量。在 1425 处观察到一个综合峰值$$厘米${}^{-1}$由于 O-H 基团的弯曲和拉伸振荡以及 zeta 电位值$=-$19.1$$毫伏。所有这些结果证实了MXene/CeCr ₂ O ₄纳米复合材料的成功形成。与单一材料相比，所得的MXene/CeCr ₂ O _{4纳米复合结构显示出显着的特性，在光学、储能和导电应用等众多应用中具有很大的潜力。}