A simple and convenient synthesis of labeled 9-hydroxy[13C6]phenanthrene as internal standard for mass spectrometry quantification of a key phenanthrene metabolite in human urines,Synthetic Communications

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A simple and convenient synthesis of labeled 9-hydroxy[13C6]phenanthrene as internal standard for mass spectrometry quantification of a key phenanthrene metabolite in human urines
Synthetic Communications ( IF 2.1 ) Pub Date : 2023-12-26 , DOI: 10.1080/00397911.2023.2288913
Jean-Yves Sancéau ₁ , Éric Gaudreau ₂ , René Maltais ₁ , Donald Poirier _{1,

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Affiliation

A simple and convenient synthesis of 9-hydroxy[13C6]phenanthrene has been developed from one-ring labeled [13C6]phenanthrene in three steps, involving a copper-ethyl acetate catalyzed “Ullmann-type...

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