Organic electrochemistry has recently witnessed a renaissance in research as a green and cost-efficient method for activating small molecules. Although some of the critical challenges of batch electrosynthesis remain, flow electrosynthesis can overcome several issues arising from batch electroorganic systems, such as mass transfer, ohmic drop, and selectivity. The combination of flow technology with electrochemistry affords practitioners a very precise control over reaction conditions, thereby enhancing the reproducibility of electrochemical processes. The use of gases in chemical reactions for the synthesis of value-added fine chemicals is of great significance. This review summarizes recent advances in flow electrochemistry for biphasic (gas–liquid) organic synthesis. We summarise recent examples of selective hydrocarbon oxidations using oxygen gas in an electrochemical flow reactor.

中文翻译：

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连续电流流双相有机合成

有机电化学作为一种绿色且经济高效的小分子活化方法，最近见证了研究的复兴。尽管间歇式电合成仍然存在一些关键挑战，但流动电合成可以克服间歇式有机电系统产生的几个问题，例如传质、欧姆降和选择性。流动技术与电化学的结合使实践者能够非常精确地控制反应条件，从而提高电化学过程的再现性。利用气体进行化学反应对于合成高附加值精细化学品具有重要意义。本综述总结了双相（气液）有机合成的流电化学的最新进展。我们总结了在电化学流动反应器中使用氧气进行选择性碳氢化合物氧化的最新例子。