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Optimum Green Synthesis, Characterization, and Antibacterial Activity of Silver Nanoparticles Prepared from an Extract of Aloe fleurentinorum
International Journal of Chemical Engineering ( IF 2.7 ) Pub Date : 2024-2-26 , DOI: 10.1155/2024/2804165
Yasmin M. S. Jamil 1 , Ahmed N. Al-Hakimi 2, 3 , Hussein M. A. Al-Maydama 1 , Ghadeer Y. Almahwiti 1 , Ashwaq Qasem 4 , Sayed M. Saleh 2, 5
Affiliation  

The synthesis of metal nanoparticles through the use of plant extract is a process that is not only simple but also inexpensive, quick, and favorable to the environment. As a result, it is utilized in a wide variety of fields. When synthesizing silver nanoparticles (AgNPs), several different kinds of plant extracts were utilized. The manufacture of silver nanoparticles was carried out in this study using an environmentally friendly technique. The aqueous extract of the Aloe fleurentinorum plant was utilized as a stabilizing and reducing agent. To determine the optimal conditions for the synthesis of silver nanoparticles, it was necessary to investigate the impact of several parameters on the process. These parameters included the reactant volume ratio, pH values, temperature, and reaction time. To get crystallite and stable silver nanoparticles, an aqueous solution of AgNO3 (0.01M) was added to an aqueous extract of Aloe fleurentinorum plant at a temperature of 60 degrees Celsius and a pH of 8. The mixture was then stirred with a magnetic stirrer for ninety minutes (90 minutes). Using a variety of methods (UV-vis spectrophotometer, FTIR, XRD, SEM, EDX, and XPS), several approaches were utilized to investigate and describe the green-produced AgNPs. Through the use of the SEM method, it was demonstrated that the morphology of AgNPs is tetrahedral. It was determined using X-ray diffraction that the size of crystalline AgNPs was 26.7 nm. AgNPs that have been optimally synthesized have antibacterial properties that are both significant and effective against various bacterial species that have been tested at varying doses.

中文翻译:

芦荟提取物制备的银纳米粒子的最佳绿色合成、表征和抗菌活性

利用植物提取物合成金属纳米粒子的过程不仅简单,而且廉价、快速且对环境有利。因此,它被广泛应用于各个领域。合成银纳米粒子(AgNP)时,使用了几种不同种类的植物提取物。本研究采用环保技术制造银纳米颗粒。芦荟植物的水提取物被用作稳定剂和还原剂。为了确定银纳米颗粒合成的最佳条件,有必要研究几个参数对过程的影响。这些参数包括反应物体积比、pH值、温度和反应时间。为了获得微晶和稳定的银纳米粒子,在60摄氏度和pH为8的温度下将AgNO 3 (0.01M)的水溶液添加到芦荟植物的水提取物中。然后用磁力搅拌器搅拌混合物九十分钟(90 分钟)。使用多种方法(紫外可见分光光度计、FTIR、XRD、SEM、EDX 和 XPS),采用多种方法来研究和描述绿色生产的 AgNP。通过SEM方法证明AgNPs的形貌为四面体。使用X射线衍射测定结晶AgNP的尺寸为26.7 nm。经过最佳合成的 AgNP 具有抗菌特性,经不同剂量的测试,这些特性对各种细菌物种均具有显着且有效的作用。
更新日期:2024-02-27
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