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Effect of compatibilizer and polyhedral oligomeric silsesquioxane on mechanical, thermal, and morphological properties of polyamide6/poly (ethylene-co-vinyl acetate) composites
Journal of Reinforced Plastics and Composites ( IF 3.1 ) Pub Date : 2024-02-26 , DOI: 10.1177/07316844241235438 Gholamreza Maghamirad 1 , Morteza Ghorbanzadeh Ahangari 2 , Majid Karimi 3 , Mostafa Hassani Niaki 2
Journal of Reinforced Plastics and Composites ( IF 3.1 ) Pub Date : 2024-02-26 , DOI: 10.1177/07316844241235438 Gholamreza Maghamirad 1 , Morteza Ghorbanzadeh Ahangari 2 , Majid Karimi 3 , Mostafa Hassani Niaki 2
Affiliation
The mechanical properties and morphology of polyamide 6/maleic anhydride grafted ethylene-co-vinyl acetate (PA6/EVA-g-MA) ternary composites are considered a function of compatibilizer (EVA-g-MA) amount at a mixing combination of 20 wt% dispersed phase (combination of EVA and the compatibilizer). 1–7 wt% compatibilizer are added to PA6/EVA-g-MA, whereas the PA6 doping is kept constant at 80 wt% in the ternary composites. Furthermore, 0.5, 1, 3, and 5 wt% octa-Isobutyl POSS (OIP) is used for reinforcement. The thermal, mechanical, and morphological properties of PA6/EVA-g-MA composites have been studied through DSC, TGA, DMTA, traditional mechanical measurements, and SEM. Tensile strength and Young’s modulus declined by increasing the compatibilizer concentration. The impact strength of PA6/compatibilizer improved considerably up to 3 wt% of the compatibilizer and then decreased. TGA analysis demonstrated a considerable improvement in the thermal stabilities of the nanocomposites by raising the OIP amount. The results of DMTA, including Tg , and DSC analysis demonstrated that the inclusion of OIP in PA6/compatibilizer considerably changed the thermal properties of only PA6 in PA6/compatibilizer. Incorporating OIP into the composite up to 1 wt% improved its modulus, tensile, and impact strength.
中文翻译:
增容剂和多面体低聚倍半硅氧烷对聚酰胺6/聚(乙烯-共-乙酸乙烯酯)复合材料机械、热和形态性能的影响
聚酰胺 6/马来酸酐接枝乙烯-醋酸乙烯酯 (PA6/EVA-g-MA) 三元复合材料的机械性能和形貌被认为是 20 wt 混合组合下增容剂 (EVA-g-MA) 用量的函数%分散相(EVA 和增容剂的组合)。PA6/EVA-g-MA 中添加了 1–7 wt% 的增容剂,而三元复合材料中 PA6 的掺杂量保持在 80 wt%。此外,还使用 0.5、1、3 和 5 wt% 八异丁基 POSS (OIP) 进行增强。通过 DSC、TGA、DMTA、传统机械测量和 SEM 研究了 PA6/EVA-g-MA 复合材料的热、机械和形态性能。通过增加增容剂浓度,拉伸强度和杨氏模量下降。PA6/增容剂的冲击强度在增容剂含量达到 3 wt% 时显着提高,然后下降。TGA 分析表明,通过提高 OIP 用量,纳米复合材料的热稳定性得到了显着改善。DMTA的结果,包括TG ,DSC 分析表明,PA6/增容剂中添加 OIP 显着改变了 PA6/增容剂中仅 PA6 的热性能。在复合材料中加入高达 1 wt% 的 OIP 可提高其模量、拉伸强度和冲击强度。
更新日期:2024-02-26
中文翻译:
增容剂和多面体低聚倍半硅氧烷对聚酰胺6/聚(乙烯-共-乙酸乙烯酯)复合材料机械、热和形态性能的影响
聚酰胺 6/马来酸酐接枝乙烯-醋酸乙烯酯 (PA6/EVA-g-MA) 三元复合材料的机械性能和形貌被认为是 20 wt 混合组合下增容剂 (EVA-g-MA) 用量的函数%分散相(EVA 和增容剂的组合)。PA6/EVA-g-MA 中添加了 1–7 wt% 的增容剂,而三元复合材料中 PA6 的掺杂量保持在 80 wt%。此外,还使用 0.5、1、3 和 5 wt% 八异丁基 POSS (OIP) 进行增强。通过 DSC、TGA、DMTA、传统机械测量和 SEM 研究了 PA6/EVA-g-MA 复合材料的热、机械和形态性能。通过增加增容剂浓度,拉伸强度和杨氏模量下降。PA6/增容剂的冲击强度在增容剂含量达到 3 wt% 时显着提高,然后下降。TGA 分析表明,通过提高 OIP 用量,纳米复合材料的热稳定性得到了显着改善。DMTA的结果,包括T