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Sonochemical Synthesis of MnFe2O4 Spinel Nanoparticles
Materials Science ( IF 0.9 ) Pub Date : 2024-04-23 , DOI: 10.1007/s11003-024-00802-w
Yu. V. Sukhatskiy , M. V. Shepida , S. A. Korniy

MnFe2O4 spinel nanoparticles were synthesized by the sonochemical method (co-precipitation in an ultrasonic field). The Bragg diffraction peaks of the synthesized product agreed with the MnFe2O4 spinel reference model, and the average MnFe2O4 crystallite size, calculated using the Debye–Scherrer equation, was approx. 7 nm. The obtained MnFe2O4 spinel nanoparticles were used as potassium persulfate activators during the oxidative degradation of the safranin T diazine dye. The degradation degree of safranin T for the duration of the “advanced” oxidation “ultrasound/ MnFe2O4 / K2S2O8 ” of 7200 s and a catalyst content of 0.1 g/L was equal to 98.3%, and the rate constant was 1.529×10–3 s–1 .



中文翻译:

MnFe2O4尖晶石纳米粒子的声化学合成

采用声化学法(超声场共沉淀)合成了MnFe 2 O 4尖晶石纳米粒子。合成产物的布拉格衍射峰与MnFe 2 O 4尖晶石参考模型一致,并且使用Debye-Scherrer方程计算的平均MnFe 2 O 4微晶尺寸约为。 7纳米。所获得的MnFe 2 O 4尖晶石纳米粒子在番红T二嗪染料的氧化降解过程中用作过硫酸钾活化剂。 “高级”氧化“超声波/MnFe 2 O 4 /K 2 S 2 O 8 ”持续时间7200 s、催化剂含量0.1 g/L时,番红T的降解程度为98.3%,速率常数为1.529×10 –3 s –1

更新日期:2024-04-24
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