Skip to main content
Log in

The Influence of Direct Laser Deposition on the Structure and Properties of Ni–Cr–W–Mo Heat-Resistant Nickel Alloy

  • PHYSICAL METALLURGY AND HEAT TREATMENT
  • Published:
Russian Journal of Non-Ferrous Metals Aims and scope Submit manuscript

Abstract

The quality of metal powder composition (MPC) made of heat resistant alloy EP648 (Ni–Cr–W–Mo) used for fabrication of parts by direct metal deposition (DMD technology) has been analyzed. It has been established that, regarding the main requirements (chemical composition, particle size distribution, purity, bulk density, yield, moisture content), the MPC meets the requirements of Technical Specifications TU 136-225-2019. The influence of the parameters of direct laser deposition (power of laser radiation, cladding speed) on the structure and microhardness of experimental specimens has been analyzed. The highest number of defects (multiple shrinkage cavities and incomplete fusion) is formed in the specimen fabricated at the power of laser radiation P = 1000 W and the cladding speed v = 40 mm/s. At the same time, the defects have the maximum dimensions. The minimum number of defects is observed in the specimens fabricated at P = 1400 and 1600 W and v = 45 and 38 mm/s. In this case, the most homogeneous structure of laser cladding is formed owing to complete fusion of powder particles and melt spreading. Nevertheless, the structure of the specimen deposited at P = 1600 W and v = 38 mm/s contains cracks located at the subgrain boundaries in the center of cladding tracks. Their formation is caused by overheating of the metal due to higher power of laser radiation and accumulation of high internal stresses after previously deposited layers. The microhardness of the specimens fabricated by all modes of direct laser deposition changes insignificantly in the range of 270–310 HV. On the basis of the obtained experimental results, it has been determined that the most optimum structure is formed in the specimen at the laser power of 1400 W and the cladding speed of 45 mm/s.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1.
Fig. 2.
Fig. 3.
Fig. 4.
Fig. 5.
Fig. 6.
Fig. 7.
Fig. 8.

Similar content being viewed by others

REFERENCES

  1. Bourell, D.L., Beaman, J.J., Wohlers, T., Frazier, W., Kuhn, H., and Seifi, M., History of additive manufacturing, in Additive Manufacturing Processes, ASM Int., 2020, vol. 24., pp. 1–8.

    Book  Google Scholar 

  2. Hopkinson, N., Hague, R.J.M., and Dickens, P.M., Rapid Manufacturing: An Industrial Revolution for the Digital Age, Chichester: John Wiley and Sons, 2006.

    Google Scholar 

  3. Attaran, M., The rise of 3-D printing: The advantages of additive manufacturing over traditional manufacturing, Bus. Horiz., 2017, vol. 60, no. 5, pp. 677–688.

    Article  Google Scholar 

  4. Gradl, P., Greene, S.E., Protz, Ch., Bullard, B., and Buzzell, J., Additive manufacturing of liquid rocket engine combustion devices: A summary of process developments and hot-fire testing results, Proc. ASEE Joint Propulsion Conference, Session: Additive Manufacturing for Propulsion Systems I, Cincinnati, OH, July 9–11, 2018, AIAA 2018-4625, pp.1–34.

  5. Ngo, T.D., Kashani, A., Imbalzano, G., Nguyen, K.T.Q., and Hui, D., Additive manufacturing (3D printing): A review of materials, methods, applications and challenges, Composites, Part B, 2018, vol. 143, no. 15, pp. 172–196.

    Article  CAS  Google Scholar 

  6. Dutta Bhaskar, Palaniswamy, S., Choi Juneho, Song Lijun, and Mazumder Jyoti, Additive manufacturing by direct metal deposition, Adv. Mater. Processes, 2011, vol. 169, pp. 33–36.

    Google Scholar 

  7. Niu, X., Singh, S., Garg, A., Singh, H., Panda, B., Peng, X., and Zhang, Q., Review of materials used in laser-aided additive manufacturing processes to produce metallic products, Front. Mech. Eng., 2019, no. 14, pp. 282–298.

  8. Pinkerton, A.J., Laser direct metal deposition: Theory and applications in manufacturing and maintenance, in Advances in Laser Materials Processing, Coventry: Woodhead Publ., 2010, pp. 461–491.

    Google Scholar 

  9. Khakimov, A.M., Zhatkin, S.S., and Shchedrin, E.Yu., Investigation of the structure and properties of parts made of heat-resistant alloys obtained by direct laser growing technology, Izv. Samar. Nauchn. Tsentra Ross. Akad. Nauk, 2020, vol. 22, no. 2, pp. 59–66.

    Google Scholar 

  10. Bo Chen, Xin Xi, Tao Gu, Caiwang Tan, and Xiaoguo Song, Influence of heat treatment on microstructure evolution and mechanical properties of TiB2/Al 2024 composites fabricated by directed energy deposition, J. Mater. Res. Technol., 2020, vol. 9, no. 6, pp. 14223–14236.

    Article  CAS  Google Scholar 

  11. Xiaoqiang Zhang, Ze Chai, Huabin Chena, Luming Xu, Hao Lu, and Xiaoqi Chen, A novel method to prevent cracking in directed energy deposition of Inconel 738 by in-situ doping Inconel 718, Mater. Des., 2021, vol. 197, article no. 109214.

    Article  CAS  Google Scholar 

  12. Girshov, V.L., Kotov, S.A., and Tsemenko, V.N., Sovremennye tekhnologii v poroshkovoi metallurgii. Uchebnoe posobie (Modern Technologies for Powder Metallurgy. Student’s Book), St. Petersburg: Peter the Great St. Petersburg Polytechnic Univ., 2010.

  13. Zhi-Yu Han, Ping-Xiang Zhang, Li-Ming Lei, Shu-Jin Liang, Qing-Xiang Wang, Yun-Jin Lai, and Jin-Shan Li, Morphology and particle analysis of the Ni3Al-based spherical powders manufactured by supreme-speed plasma rotating electrode process, J. Mater. Res. Technol., 2020, vol. 9, no. 6, pp. 13937–13944.

    Article  CAS  Google Scholar 

  14. Kaplanskii, Yu.Yu., Zaitsev, A.A., Sentyurina, Zh.A., Levashov, E.A., Pogozhev, Yu.S., Loginov, P.A., and Logachev, I.A., The structure and properties of pre-alloyed NiAl–Cr(Co,Hf) spherical powders produced by plasma rotating electrode processing for additive manufacturing, J. Mater. Res. Technol., 2018, vol. 7, no. 4, pp. 461–468.

    Article  CAS  Google Scholar 

  15. Zhong, Ch., Chen, J., Linnenbrink, S., Gasser, A., Sui, Sh., and Poprawe, R., A comparative study of Inconel 718 formed by high deposition rate laser metal deposition with GA powder and PREP powder, Mater. Des., 2016, vol. 107, pp. 386–392.

    Article  CAS  Google Scholar 

  16. Zhang, Y., Li, Z., Nie, P., and Wu, Y., Effect of cooling rate on the microstructure of laser-remelted Inconel 718 coating, Metall. Mater. Trans. A, 2013, vol. 44, pp. 5513–5521.

    Article  CAS  Google Scholar 

  17. Lee, Y., Nordin, M., Babu, S.S., and Farson, D.F., Effect of fluid convection on dendrite arm spacing in laser deposition, Metall. Mater. Trans. B, 2014, vol. 45, pp. 1520–1529.

    Article  CAS  Google Scholar 

  18. Sui, S., Chen, J., Ming, X.L., Zhang, S.P., Lin, X., and Huang, W.D., The failure mechanism of 50% laser additive manufactured Inconel 718 and the deformation behavior of Laves phases during a tensile process, Int. J. Adv. Manuf. Technol., 2017, vol. 91, pp. 2733–2740.

    Article  Google Scholar 

  19. Parimi, L.L., Ravi, G.A., Clark, D., and Attallah, M.M., Microstructural and texture development in direct laser fabricated IN718, Mater. Charact., 2014, vol. 89, pp. 102–111.

    Article  CAS  Google Scholar 

  20. Tammas-Williams, S., Withers, P.J., Todd, I., and Prangnell, P.B., The influence of porosity on fatigue crack initiation in additively manufactured titanium components, Sci. Rep., 2017, no. 7, pp. 1–13.

  21. Farber, B., Small, K.A., Allen, C., Causton, R.J., Nichols, A., Simbolick, J., and Taheri, M.L., Correlation of mechanical properties to microstructures in Inconel 718 fabricated by direct metal laser sintering, Mater. Sci. Eng., A, 2018, vol. 712, pp. 539–547.

    Article  CAS  Google Scholar 

  22. Sui, S., Tan, H., Chen, J., Zhong, Ch., Li, Z., Fan, W., Gasser, A., and Huang, W., The influence of laves phases on the room temperature tensile properties of Inconel 718 20 fabricated by powder feeding laser additive manufacturing, Acta Mater., 2019, vol. 164, pp. 413–427.

    Article  CAS  Google Scholar 

  23. Konovalov, S., Osintsev, K., Golubeva, A., Smelov, V., Ivanov, Yu., Chen, X., and Komissarova, I., Surface modification of Ti-based alloy by selective laser melting of Ni-based superalloy powder, J. Mater. Res. Technol., 2020, vol. 9, no. 4, pp. 8796–8807. https://doi.org/10.1016/j.jmrt.2020.06.016

    Article  CAS  Google Scholar 

  24. Ageev, E.V., Ageeva, E.V., and Altukhov, A.Yu., A Study of the structure and properties of hardened additive articles obtained from electroerosion cobalt-chromium powder, Met. Sci. Heat Treat., 2021, vol. 63, nos. 3–4, pp. 210–213. https://doi.org/10.1007/s11041-021-00672-y

    Article  CAS  Google Scholar 

  25. Qian, S., Dai, Y., Guo, Y., and Zhang, Y., Microstructure and wear resistance of multi-layer Ni-based alloy cladding coating on 316L SS under different laser power, Materials, 2021, vol. 14, no. 4, article no. 781. https://doi.org/10.3390/ma14040781

    Article  CAS  Google Scholar 

Download references

Funding

This work was supported by the Ministry of Education and Science of the Russian Federation, governmental project no. 0778-2020-0005.

Author information

Authors and Affiliations

Authors

Corresponding authors

Correspondence to A. M. Khakimov, S. S. Zhatkin, K. V. Nikitin, V. I. Nikitin or V. B. Deev.

Ethics declarations

The authors declare that they have no conflicts of interest.

Additional information

Translated by I. Moshkin

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Khakimov, A.M., Zhatkin, S.S., Nikitin, K.V. et al. The Influence of Direct Laser Deposition on the Structure and Properties of Ni–Cr–W–Mo Heat-Resistant Nickel Alloy. Russ. J. Non-ferrous Metals 63, 305–314 (2022). https://doi.org/10.3103/S1067821222030075

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.3103/S1067821222030075

Keywords:

Navigation