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X-ray powder diffraction data for three new compounds obtained as a result of CO2 capture

Published online by Cambridge University Press:  23 November 2023

Klaudia Nowakowska Open the ORCID record for Klaudia Nowakowska [Opens in a new window]  and
Wiesław Łasocha Open the ORCID record for Wiesław Łasocha [Opens in a new window]
Klaudia Nowakowska
Affiliation:
Faculty of Chemistry, Jagiellonian University, Gronostajowa 2, 30-387 Krakow, Poland
Wiesław Łasocha*
Affiliation:
Faculty of Chemistry, Jagiellonian University, Gronostajowa 2, 30-387 Krakow, Poland Jerzy Haber Institute of Catalysis and Surface Chemistry PAS, Niezapominajek 8, 30-239 Krakow, Poland
*
a)Author to whom correspondence should be addressed. Electronic mail: lasocha@chemia.uj.edu.pl
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Abstract

The field of research related to CO2 capture is significant and really attractive for sustainable green chemistry. Focusing attention on this topic in our research led to obtaining new compounds based on diamines. As a result of the syntheses carried out using aqueous solutions of diamines exposed to the slow action of carbon dioxide from the air, three new monocarbamates were obtained. X-ray powder diffraction data for the obtained compounds: 12-propCO2 (C4H10N2O2) [a = 9.3033(7), b = 9.2485(7), c = 7.4735(7) Å, β = 111.214(7)°, V = 599.46 Å3, Z = 4, space group Ia]; 13-propCO2 (C4H10N2O2) [a = 5.0065(10), b = 12.2093(23), c = 4.9006(10) Å, β = 96.457(18)°, V = 297.65 Å3, Z = 2, space group P21]; and 13-dytekCO2 (C6H14N2O2) [a = 28.374(3), c = 5.1726(9) Å, V = 3606.53 Å3, Z = 18, space group $R\bar{3}$] are reported in this paper.

Keywords

carbamateCO2 capturealiphatic aminesX-ray diffraction
Type
New Diffraction Data
Information
Powder Diffraction , Volume 38 , Issue 4 , December 2023 , pp. 253 - 258
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Copyright
Copyright © The Author(s), 2023. Published by Cambridge University Press on behalf of International Centre for Diffraction Data

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