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Synthesis and High-Temperature Heat Capacity of LaMgAl11O19 and SmMgAl11O19 Hexaaluminates

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Abstract

The processes occurring during heating of a stoichiometric mixture of lanthanum, samarium, magnesium, and aluminum hydroxides synthesized by the reverse precipitation method have been studied by DTA/TG and X-ray powder diffraction methods. The conditions for the synthesis of single-phase LaMgAl11O19 and SmMgAl11O19 samples of the magnetoplumbite structure type have been determined, and the isobaric heat capacity has been measured in the temperature range 317–1817 K, showing the absence of structural transformations in this range.

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Funding

The study was supported by the Russian Science Foundation (project no. 23-13-00051), https://rscf.ru/project/23-13-00051/, with the use of equipment of the Joint Research Center for Physical Methods of Investigation, Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences.

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Authors and Affiliations

  1. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, 119991, Moscow, Russia

    P. G. Gagarin, A. V. Guskov, V. N. Guskov, A. V. Khoroshilov, M. A. Ryumin & K. S. Gavrichev

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  1. P. G. Gagarin
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  2. A. V. Guskov
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  3. V. N. Guskov
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  4. A. V. Khoroshilov
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  5. M. A. Ryumin
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  6. K. S. Gavrichev
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Correspondence to P. G. Gagarin.

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Translated by G. Kirakosyan

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Gagarin, P.G., Guskov, A.V., Guskov, V.N. et al. Synthesis and High-Temperature Heat Capacity of LaMgAl11O19 and SmMgAl11O19 Hexaaluminates. Russ. J. Inorg. Chem. 68, 1599–1605 (2023). https://doi.org/10.1134/S0036023623602064

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  • DOI: https://doi.org/10.1134/S0036023623602064

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