Abstract
A new method for producing highly dispersed strontium aluminate with specified properties (low bulk density, particle size and shape) is described. The essence of the method is the sequential multi-stage heat treatment of a concentrated water-carbohydrate solution of Al(NO3)3, Sr(NO3)2, and D-glucose. The final product has a molar ratio of SrO : Al2O3 = 1 : 1. The main stages of the synthesis have been characterized by X-ray powder diffraction, SEM, and TEM methods. The initial stages of crystallization of SrAl2O4 upon heating at 1400°C have been revealed.
Similar content being viewed by others
REFERENCES
P. Ptáček, F. Šoukal, T. Opravil, et al., Ceram. Int. 40, 9971 (2014). https://doi.org/10.1016/j.ceramint.2014.02.095
B. M. J. Smets, Mater. Chem. Phys. 16, 283 (1987). https://doi.org/10.1016/0254-0584(87)90103-9
T. A. Khattab, M. Rehan, Y. Hamdy, et al., Ind. Eng. Chem. Res. 57, 11483 (2018). https://doi.org/10.1021/acs.iecr.8b01594
D. G. Calatayud, T. Jardiel, E. Cordero-Oyonarte, et al., Int. J. Mol. Sci. 23, 3410 (2022). https://doi.org/10.3390/ijms23063410
D. Madej, M. Silarski, and S. Parzych, Mater. Chem. Phys. 260, 124095 (2021). https://doi.org/10.1016/j.matchemphys.2020.124095
F. Clabau, X. Rocquefelte, S. Jobic, et al., Chem. Mater. 17, 3904 (2005). https://doi.org/10.1021/cm050763r
S. Sharma, J. James, S. Gupta, et al., Materials 16, 236 (2023). https://doi.org/10.3390/ma16010236
H. Tseng, W. Tzou, S. Wei, et al., J. Mater. Res. Technol. 9, 14051 (2020). https://doi.org/10.1016/j.jmrt.2020.10.003
H. Terraschke, M. Suta, M. Adlung, et al., J. Spectrosc. (Hindawi) 2015, 1 (2015). https://doi.org/10.1155/2015/541958
J. Li, J. Wang, Y. Yu, et al., J. Rare Earths 35, 530 (2017). https://doi.org/10.1016/S1002-0721(17)60944-X
Y. Zhang, L. Li, X. Zhang, et al., J. Rare Earths 26, 656 (2008). https://doi.org/10.1016/S1002-0721(08)60156-8
Y. Jin, X. Long, Y. Zhu, et al., J. Rare Earths 34, 1206 (2016). https://doi.org/10.1016/S1002-0721(16)60155-2
L. Chen, Z. Zhang, Y. Tian, et al., J. Rare Earths 35, 127 (2017). https://doi.org/10.1016/S1002-0721(17)60890-1
R. Zhao, R. Pang, H. Li, et al., J. Rare Earths 32, 797 (2014). https://doi.org/10.1016/S1002-0721(14)60143-5
A. Kumar, G. Kedawat, P. Kumar, et al., New J. Chem. 39, 3380 (2015). https://doi.org/10.1039/c4nj02333a
J. Xu and S. Tanabe, J. Lumin. 205, 581 (2019). https://doi.org/10.1016/j.jlumin.2018.09.047
V. Castaing, E. Arroyo, A. Becerro, et al., J. Appl. Phys. 130, 080902 (2021). https://doi.org/10.1063/5.0053283
A. Ege and S. Yerci, et al., J. Lumin. 131, 2432 (2011). https://doi.org/10.1016/j.jlumin.2011.05.051
R. E. Rojas-Hernandez, M. A. Rodriguez, F. Rubio-Marcos, et al., J. Mater. Chem. C 3, 1268 (2015). https://doi.org/10.1039/c4tc02262a
T. A. Kochergina, S. S. Aleshkina, M. M. Khudyakov, et al., Quantum Electron. 48, 733 (2018). https://doi.org/10.1070/QEL16740
I. V. Kozerozhets, G. P. Panasyuk, E. A. Semenov, et al., Ceram. Int. 48, 7522 (2022). https://doi.org/10.1016/j.ceramint.2021.11.296
G. P. Panasyuk, I. V. Kozerozhets, E. A. Semenov, et al., Inorg. Mater. 55, 929 (2019). https://doi.org/10.1134/S0020168519090139
I. I. Buchinskaya and N. I. Sorokin, Russ. J. Inorg. Chem. (2023). https://doi.org/10.1134/S0036023623600806
A. Y. Solovieva, Y. V. Ioni, A. O. Baskakov, et al., Russ. J. Inorg. Chem. 62, 711 (2017). https://doi.org/10.1134/S0036023617060225
S. H. Tatumi, A. Soares, D. R. G. Tudela, et al., Radiat. Phys. Chem. 157, 15 (2019). https://doi.org/10.1016/j.radphyschem.2018.12.013
N. I. Steblevskaya, M. V. Belobeletskaya, M. A. Medkov, et al., Russ. J. Inorg. Chem. 62, 275 (2017). https://doi.org/10.1134/S0036023617030160
M. Sera, M. Yamamoto, K. Tomita, et al., Chem. Phys. Lett. 780, 138916 (2021). https://doi.org/10.1016/j.cplett.2021.138916
I. V. Kozerozhets, V. V. Avdeeva, G. A. Buzanov, et al., Inorganics 10, 212 (2022). https://doi.org/10.3390/inorganics10110212
I. V. Kozerozhets, G. P. Panasyuk, E. A. Semenov, et al., Powder Technol. 413, 118030 (2023). https://doi.org/10.1016/j.powtec.2022.118030
K. T. Jacob and V. Shreyas, J. Mater. Sci. 53, 1723 (2017). https://doi.org/10.1007/s10853-017-1634-0
S. Kim, H. Won, N. Hayk, et al., Mater. Sci. Eng. B 176, 1521 (2011). https://doi.org/10.1016/j.mseb.2011.09.014
C.-N. Xu, H. Yamada, X. Wang, et al., Appl. Phys. Lett. 84, 3040 (2004). https://doi.org/10.1063/1.1705716
I. V. Kozerozhets, G. P. Panasyuk, E. A. Semenov, et al., Russ. J. Inorg. Chem. 65, 1384 (2020). https://doi.org/10.1134/S0036023620090090
ACKNOWLEDGMENTS
X-ray diffraction studies were carried out using the equipment of the Center for Collective Use of the Physical Research Methods at the Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences. For SEM studies, we used the equipment of the Educational and Methodological Center for Lithography and Microscopy of the Moscow State University.
Funding
This work was carried out within the framework of the State Assignment of the Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences in the field of fundamental scientific research.
Author information
Authors and Affiliations
Corresponding author
Ethics declarations
The authors declare that they have no conflicts of interest.
Additional information
Translated by V. Avdeeva
Publisher’s Note.
Pleiades Publishing remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
About this article
Cite this article
Kozlova, L.O., Ioni, Y.V., Son, A.G. et al. Low-Temperature Synthesis of Highly Dispersed Strontium Aluminate. Russ. J. Inorg. Chem. 68, 1744–1751 (2023). https://doi.org/10.1134/S0036023623602374
Received:
Revised:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S0036023623602374