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Dispersive and Magnetic Solid-Phase Extraction of Organic Compounds: Review of Reviews

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Abstract

Dispersive solid-phase extraction (DSPE) and magnetic solid-phase extraction (MSPE) are methods of solid-phase sorption preconcentration. Compared to classical solid-phase extraction, these methods have a number of advantages, such as reduced consumption of sorbents and solvents, extraction time, and cost of analysis. The popularity of the method among the analysts is evidenced by the large number of reviews we have summarized in this publication. Information is systematized on different versions of these methods, differing in the way the preconcentration process is carried out, the nature of the sorbents used, and their combination with methods for the subsequent determination of the preconcentrated substances; examples of using DSPE and MSPE for the separation of organic compounds in the analysis of environmental samples, food products and biological fluids are given.

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Funding

The work was carried out within the framework of the State Assignment, topic no. AAAA-A21-121011990021-7. The authors express their gratitude to the Interdisciplinary Scientific and Educational School of Moscow University “The Future of the Planet and Global Environmental Changes.”

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Dmitrienko, S.G., Apyari, V.V., Tolmacheva, V.V. et al. Dispersive and Magnetic Solid-Phase Extraction of Organic Compounds: Review of Reviews. J Anal Chem 79, 105–118 (2024). https://doi.org/10.1134/S1061934824020060

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