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Licensed Unlicensed Requires Authentication Published online by De Gruyter February 29, 2024

Synthesis and structure of a manganese(II) coordination polymer assembled with 5-(tert-butyl)isophthalic acid and 1,3-dimethyl-2-imidazolidinone

  • Xin-hong Chang EMAIL logo
From the journal Zeitschrift für Naturforschung B
https://doi.org/10.1515/znb-2022-0093

Abstract

A manganese(II) coordination polymer [Mn(tbip)(DMI)] n (1), (tbipH2 = 5-(tert-butyl)isophthalic acid, DMI = 1,3-dimethyl-2-imidazolidinone), has been synthesized under “urea-thermal conditions” (i.e. in an excess of urea). Its structure has been determined by single-crystal X-ray diffraction analysis and further characterized by elemental analysis and IR spectra. Complex 1 crystallizes in the monoclinic space group P21/c with Z = 4. In 1, the [tbip]2− ligand bridges the Mn(II) cations to form infinite chains, and the neighbouring chains are connected through [tbip]2− ligands into layers.

Keywords: manganese complex; isophthalate ligands; urea ligands; coordination polymer; crystal structure
Corresponding author: Xin-hong Chang, College of Chemistry and Chemical Engineering, Luoyang Normal University, Luoyang 471934, P.R. China, E-mail:

  1. Research ethics: Not applicable.

  2. Author contributions: The author has accepted responsibility for the entire content of this manuscript and approved its submission.

  3. Competing interests: The author states no conflict of interest.

  4. Research funding: None declared.

  5. Data availability: The raw data can be obtained on request from the corresponding author.

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Received: 2022-06-13
Accepted: 2023-08-08
Published Online: 2024-02-29

© 2024 Walter de Gruyter GmbH, Berlin/Boston

From the journal
Zeitschrift für Naturforschung B
Zeitschrift für Naturforschung B

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