Russian Journal of Inorganic Chemistry ( IF 2.1 ) Pub Date : 2023-12-28 , DOI: 10.1134/s0036023623602374 L. O. Kozlova , Yu. V. Ioni , A. G. Son , G. A. Buzanov , G. P. Murav’eva , I. V. Kozerozhets
Abstract
A new method for producing highly dispersed strontium aluminate with specified properties (low bulk density, particle size and shape) is described. The essence of the method is the sequential multi-stage heat treatment of a concentrated water-carbohydrate solution of Al(NO3)3, Sr(NO3)2, and D-glucose. The final product has a molar ratio of SrO : Al2O3 = 1 : 1. The main stages of the synthesis have been characterized by X-ray powder diffraction, SEM, and TEM methods. The initial stages of crystallization of SrAl2O4 upon heating at 1400°C have been revealed.
中文翻译:
高分散铝酸锶的低温合成
摘要
描述了一种生产具有特定性能(低堆积密度、颗粒尺寸和形状)的高度分散的铝酸锶的新方法。该方法的本质是对Al(NO 3 ) 3、Sr(NO 3 ) 2和D-葡萄糖的浓缩水-碳水化合物溶液进行顺序多级热处理。最终产物的摩尔比为SrO : Al 2 O 3 = 1 : 1。通过X射线粉末衍射、SEM和TEM方法对合成的主要阶段进行了表征。已经揭示了在 1400°C 加热时SrAl 2 O 4结晶的初始阶段。